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Rotary Evaporator

Ai 10L SolventVap w/ PolyScience Chiller & ULVAC PTFE Pump

  • Model Number:

    TMAX-10L-2
  • Net Weight:

    200 Lb (evaporator), 100 Lb (glassware)
  • Compliance:

    CE Certified
  • Warranty:

    One year limited warranty with lifetime technical support
  • Payment:

    L/C D/A D/P T/T Western Union
  • Delivery Time:

    5 days
Product Details

Ai 10L SolventVap w/ PolyScience Chiller & ULVAC PTFE Pump


A rotary evaporator is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation. The process of rotary evaporation is most often used to separate solvents with low boiling points, such a n-hexane or ethyl acetate, from compounds which are solid at room temperature and pressure. However, careful application also allows for the removal of a solvent from a sample containing a liquid compound, if there is minimal co-evaporation (azeotropic behavior) and a sufficient difference in boiling points at the chosen temperature and reduced pressure.

    

Ai SolventVap 2.6-gallon/10L (evaporating flask capacity) series rotary evaporators come with all PTFE valves for solvent-resistant operations. We also lowered the height of assembled unit, for easy installation and ease of use and storage. Also come with them are vertical glassware and digital temperature/rotation control. Its optimized bath volume allows for rapid heat-up times. The condenser unit has specially designed glass tubes that utilize surface area extremely efficiently. That’s why our SolventVap evaporators consistently deliver reliable and reproducible process results that are usually reserved for more costly systems. Another important aspect of the SolventVap is the safety features, which includes dry-run protection, water bath over-temperature shut-off protection, and fuse protection.

Rotary evaporator features a specially designed motor and worm gear, which provides constant rotation at speeds from 10 to 130 rpm. As the flask containing the solvent is rotated, it continually transfers a thin layer of liquid over the entire inner surface. This gives a very large surface area for evaporation, which is caused by the gentle heating from the water bath. The rotating system is fitted with a special seal that allows the apparatus to be placed under vacuum, effectively reducing the boiling point of the solvents and removing the vapor phase, making the process much more efficient. Each unit is also equipped with an easy-to-use vacuum release and a continuous feed system, which allows solvent to be constantly drawn into the rotating flask without needing to stop the operation.

Digital water bath operates from ambient temperature to 99°C (210°F) with PID temperature control stepping at 0.1°C increments. Heating coils are located directly inside the pan for the most efficient heating possible. A built-in overheat protector will shut down power, should the controller fail.

Standard Glassware Set includes 2.6 gallon (10 liters) round-bottomed evaporating flask, 1.3 gallon (5 liters) round-bottomed receiving flask, and vertical condenser. Rotary evaporators with vertical glass condenser are great for distillation of solvents with higher boiling points.


Features

·        Water bath cover enhances safety by protecting evaporating flask and the material inside; it gives you uniform temperature inside evaporation flask as well as energy saving by reducing heat loss. It also creates a better lab environment by preventing heat and humidity from escaping.

·        Solvent-resistant PTFE and Viton gaskets, ensuring long time operation.

·        Specialized motor with extremely compact, intermeshed worm and worm gear provides precise driving for very quiet, vibration-free operation.

·        Downward-condensing vacuum connection design ensures safe vacuum operation.

·        Motorized water bath lifting for precise control.

·        Easy, straight-forward visual operation with digital speed and temperature display.

·        PID temperature controller ensures accurate temperature control is maintained.

·        One year warranty on rotary evaporator except for glassware and all sealing gaskets.


Your safety is important to us! Please use caution when operating. Users of glass reaction equipment must take all necessary precautions to avoid contact with rotating parts, particularly entanglement of loose clothing, hair, necklaces, or other jewelry. Under these circumstances, the winding action of the rotating parts can draw the user(s) into the apparatus, resulting in breakage of glassware, burns, and/or chemical exposure. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

 

Specifications

 Electrical requirements

 220V 50/60Hz single phase, 17.3A, 3800 watt (rotation motor: 300 watts)

 Glass material

 High borosilicate glass 3.3

 Evaporating flask

 Capacity: 2.6 gallon (10 liters or 0.35 cu ft)
 Maximum load: Not to exceed 60% of the flask's capacity
 Sealing flange: 4.9" diameter
 Rotation speed: 10 to 130 rpm
 Evaporating speed: 0.75 gallon/hour (water), 1.5 gallon/hour (alcohol)

 Receiving flask

 1.3 gallon (5 liters or 0.18 cu ft)

 Condenser

 Glassware: Main + auxiliary triple-circulating cold traps, vertical
 Chilling fluid conneciton: 3/8" hose barb x 4 (2 on main + 2 on auxiliary)
 Condensing surface
   Main condenser: 3,900 cm2 or 4.2 sq ft
   Auxiliary condenser: 2,530 cm2 or 2.7 sq ft

 Working environment

 5 to 95°F

 Water bath

 Temperature range: ambient to 99°C (210°F)
 Temperature controller: digital
 Dimensions: 12.5" diameter x 8.7" depth x 11" height
 Material: stainless steel
 Media: distilled water only
 Max. water level: not to exceed 1" from the top rim of the bath
 Number of heaters: two
 Drain port: one
 Exterior liner: rubber
 Lifting: motorized
 Maximum lifting distance: 4 inches

 Vacuum

 Ultimate vacuum level: < 3 torrs
 Vacuum sealing: PTFE + Viton gaskets
 Vacuum connection: 3/8" hose barb x 1 on main condenser

 Swivel caster

 Four, built-in with locks

 Safety

 Dry-run, over-temp shut-off, built-in circuit breakers

 Weight & dimensions

 Shipping weight: 200 Lb (evaporator), 100 Lb (glassware)
 Unit dimensions: 36 x 22 x 67" (WxDxH) 
 Shipping dimensions: 39 x 22 x 44" (evaporator), 30 x 25 x 28" (glassware) (WxDxH)

 Certification

 UL, CSA

 






SE26ps Standard Package

 Part description

 Quantity

 PolyScience 220V 6160 -10°C 4.2L 1HP recirculating chiller with turbine pump

1 set

 ULVAC 220V DTC-41 1.6 cfm 7.5 torr 2-head diaphragm pump and vacuum hose

1 set 

 Ai SolventVap 2.6-gallon rotary evaporator and water bath

1 set

 Vertical main and auxiliary condensers, glass

2 pcs

 2.6G/10L round shaped rotating evaporating flask, glass

1 pc

 5L receiving flask with detachable drain port

1 pc

 Three-way tee vapor buffering flask, glass

1 pc

 Glass vapor duct with seal (pre-installed)

1 set 

 PTFE vacuum sealing kit (pre-installed)

2 pcs

 Receiving flask glass vacuum port with PTFE open/close valve

2 sets

 Glass material feeding port with PTFE open/close valve

1 set

 PTFE extension feeding hose

1 pc

 Stainless steel pole and mechanical vacuum gauge

2 pcs

 Reinforced food grade vacuum and chilling tubing

15 ft

 Rubber-wrapped condenser & receiving flask support and bracket

3 pcs

 Flask quick clamp & centering ring

7 sets

 GL18 x 5, 3/8" fluid port for C30 chillers x 2

See left

 Evaporating flask cap spanner, allen key & hex screws

1 set

 Ai plexiglass cover for SolventVap 10L

1 pc

 User's manual

1 pc